Annexure I: Technical Specifications for equipment, Testing Lab ...

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Annexure I: Technical Specifications for equipment
, Testing Lab, Kanpur


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1















BOOK
I
I







TECHNICAL SPECIFICATIONS FOR EQUIPMENT














Annexure I: Technical Specifications for equipment
, Testing Lab, Kanpur


Page
2


1.

30 kN Capacity Universal Materials Test System Specification

General

The te
sting instrument shall consist of a 30kN capacity
Load frame, a Load weighing system, and Software for
machine control, data acquisition and data
manipulation. All of these components must be fully
integrated and supported by the vendor.

Material Testin
g System Specifications


This unit shall integrate the following major sub
-
systems into a complete operating system.
The major sub
-
systems and their specifications are:

Loading Frame

The dual column
-
loading frame shall be capable of
tension, compression,

flexure, shear, and reverse stress
testing. It should include a digital closed loop
command and feedback motion control system.



The frame shall include dual level mechanical limit
switches on the front of the frame that prevent the
crosshead from travel
ing too high or too low. The
first level switch should stop the crosshead and the
second level limit switch should cut the power to
the frame should the first level limits ever fail in the
future.



The vertical distance between the top surface of the
base p
laten to the bottom surface of the moving
crosshead shall be at least 1100 mm for load cells,
grips and fixtures.



The total height of the load frame shall be a
maximum of 1580mm.



The maximum load capacity shall be at least 30kN
(3,000 kg)



Additional load
cell of 1kN, 0.5kN, 0.1kN should
be supplied along with instrument.



Wedge action grips, capacity 30kN; Faces flat
serrated, 25mm wide x 57mm high
-
1 set; Facesflat
serrated. 25mm wide x 57mm with wedge action
grips
-
1 set



Pneumatic side action grips Capacit
y: 1 kN;
required jaw faces and an air distribution kit
-
1 set




Jaw faces 25mm x 38mm ; 75mm x 25mm


1 set
each



Pneumatic footswitch, rigid coupling.



The speed range should be 0.005 mm to 500 mm
per minute and shall be settable continuously. The
return s
peed shall be 600 mm/min (24 in/min).

Annexure I: Technical Specifications for equipment
, Testing Lab, Kanpur


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The steady state speed accuracy shall be +/
-
0.2%,
of set speed measured over full speed range.



The maximum load at 500 mm/min shall be at least
30kN.



For safety purposes, the frame shall incorporate an
auto
-
frame stand
by mode that automatically stops
the frame when the transducer, interface, or
computer is disconnected or shutdown.



The frame shall include integrated T
-
slots on the
front and back of both column covers for easy
mounting of accessories.


Load Weighing Sy
stem,
Transducers & Electronics



The system should be supplied with a +/
-
30kN
capacity load cell mounted under its moving
crosshead.



Load cell and extensometer transducers available
for the system shall include self
-
identification
(recognition) electronic
s in the connector directly
attached to these transducers which automates the
calibration of these devices.



The load weighing system accuracy shall be within
+/
-
0.5% of reading down to 1/100
th

of the load cell
capacity.



Any load cell provided shall have

105% over range
protection that will stop the frame automatically.



The computer shall communicate to the frame
though an Ethernet 10/100 Mb/sec interface.



The system should have a CE certification for
susceptibility and emissions.


Software




The cont
rol software will be a true graphical user
interface meeting all of the Microsoft Windows
standards. Dos based software is not acceptable.



The software must have multi levels of user access
based on his or her login name and password.



The testing software
must be able to perform
tensile, compression, flexure, peel, tear, friction and
simple cyclic tests and include an appropriate
calculation list for each type of test.



The control software shall include set
-
up of the
following: test speed, limits on all ch
annels,
calibration and balance of transducers, specimen
dimensions, and results tables at a minimum.



An unlimited number of test methods shall be
available for storage and retrieval.



The operating software shall allow the user to select
from a list of lan
guages to be displayed



The software shall provide security based on 3
Annexure I: Technical Specifications for equipment
, Testing Lab, Kanpur


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defined user levels with password protection.



The software must include the capability to define
correction factors such as machine compliance,
slack, pretension, load and gauge length.



The ability to re
-
analyze past test data using
different calculations must be provided.



The software shall allow the user to define the
company logo on the report.



The software should have Unlimited no. of live
displays in test workspace on the test scree
n.



The software should have a provision to view the
live raw data capturing on the test screen.



The software should have a facility for the
connection of a webcam or other video capturing
device, giving the end user an ability to experience
point
-
by
-
point
playback of the specimen throughout
the test.



Software should allow the unlimited zooming in on
any detailed region of the graph.



There should be a facility for real
-
time calculations
in live displays.



The software should have a provision to program
the au
dio alerts to inform about the happening of
events during a test.



A facility to send results and reports automatically
to e
-
mail address, printer, database, network drive.



A facility to identify the transducers and link them
to methods so that there is no
error in choosing the
proper method and device.



A facility to set up a choice input with linked
parameters.



A facility to modify or add new calculation even
after the test is over and update the results and
graph.



A facility to copy the graph and result ta
ble from
software and paste them to excel and word
applications.



A facility for cyclic test that allows for building
blocks that link together and defines the test.



Auto recovery of data on power failure.


Data acquisition




Run time screen must be capabl
e of displaying both
the real time graph and the calculated results of
multiple specimens simultaneously.



The control software shall be capable of acquiring
data at 100 Hz across load, displacement, and up to
two optional strain channels. Data rates shou
ld not
be affected by the number of strain channels
Annexure I: Technical Specifications for equipment
, Testing Lab, Kanpur


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collected.



Test control software must be able to automatically
store raw data or calculated results in an ASCII file.







2.

Toe Impact Tester

Instrument Scope

To determine the impact
resistance

of
toe

ca
p
used

for
safety footwear

Impact Energy.

(EN) 200J, (BS, ANSI) 100±2J

No of striker

2

Specification

Impact apparatus, incorporating a steel striker of mass
20 kg ± 0,2 kg adapted to fall freely on vertical

guides from a predetermined height to give th
e
required impact energy. Provision should be made for a
mechanism to catch the striker after the first impact so
that the test specimen is struck only once

Power

1

,AC 220V,2A

Standard Reference

EN ISO 20344, ANSI
-
Z41,CSA
-
Z195, LD50



3.

Leakproofness Tes
ter

Instrument Scope

To assess the leak proofness of safety footwear

Specifications

Instrument incorporate with rubber collar to seal the top
edge of the test piece, through which compressed air
may be fed via appropriate connections with a
constant int
ernal pressure of (10 ± 1) kPa for 30 s.

Standard Reference

EN ISO 20344.5.7




4.

Bally Flex Meter


Instrument Scope

Suitable device to test thin leather products for vamp, dress
cloth and bags leather flexing

Specifications

No of Grips:
12

The upper

clamp can be reciprocated by
a motor about a
horizontal axle
, descending through an angle of 22° 30’ ± 0° 30’
Annexure I: Technical Specifications for equipment
, Testing Lab, Kanpur


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at

a frequency of 100 cycles/min ± 5 cycles/min.

LCD counter: 0~999,999

Additional requirement:
Press knife
, conforming to the
requirements o
f ISO 2419, the inner wall of which is a rectangle
70 mm ± 1 mm x 45 mm ± 1 mm.

Magnifier
, with a magnification of 4 to 6 times
.

Power: 1

,AC 220V,3A

Standard Reference

EN ISO 5402, IUP 10,JIS K6545






5.

Water Vapour Tester (WVP)

Instrument Scope

To analyse the water vapour permeability of leather, industrial
fabrics and all permeable materials

Specifications

Sample rotation speed 75+
-

5

rpm

Ventilation system: 3 blades rotating at 1400 ±100 rpm

Assembly with rotating beaker holder for 6 positions with rapid
release system

6 glass breakers

Protection system for the operator

Power:
220v
-
50Hz

Standard Reference

EN ISO 20344, ISO
EN 14268, EN 420



6.

Vamp
Flex Tester

Instrument Scope

A machine used to assess the tendency of all type of shoe upper
materials, clothing leathers and upholstery coverings to crack or
break as a result of flexing in wear.


Specifications

No of station: 12

Interlocked guarding

To include multi function operation and display module that
automatically adjusts incoming electrical supply

Inner compartment with cooling facility to reach up to minus 10
deg Celsius

Cycle Rate 300 / min

Jog facility; Clam
p operation for holding of samples

Standard Reference

SATRA TM 25, ISO 4643 (Annex B)



Annexure I: Technical Specifications for equipment
, Testing Lab, Kanpur


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7.


Martindale Abrasion Tester

Instrument Scope

To test the leather , textile material for abrasion testing


Specifications



No of specimen : 9



Expose area of specimen:

6.45 cm² for abrasion & 64.5 cm²
for pilling of textile material



Working pressure on test specimen: 9kPa & 12 kPa



Rotation speed: 47.5±2.5 rpm



Total stroke of derive unit: 60.5±0.5mm



Parallelism of top plate to abrading tables: ≤0.05mm



Parallelism of samp
le holder to abrading tables: ≤0.05mm



Dimensions of the Lissajous figure: (60 ± 1) mm




Symmetry of Lissajous figure: Curves shall be parallel and
evenly spaced




Face diameter of specimen holder insert: (28,65 ± 0,25) mm



Combined mass of specimen holder, sp
indle and weight:

( 795
±

Standard Reference



EN ISO 20344(6.12),EN ISO 12947, EN 388, ISO 17704



8.

Thickness Gauge Tester

Instrument Scope

To test the thickness of the leather


Specifications



Anvil diameter 10mm



Presser foot diameter 10mm



App
lied pressure 49+/
-
5 kPa



Digital display



Lever operation of lowering weighted arm

Standard Reference



SATRA TM 1, ISO 2589



9.

Water Absorption & Desorption

Instrument Scope

To determine the water absorption & desorption of insole &
insock material of safet
y footwear.

Specification

Speed: 20 ± 1 cycles / min

Stroke : 50 ± 1 mm

Annexure I: Technical Specifications for equipment
, Testing Lab, Kanpur


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Compression load: 80 ± 5N

Water Flow rate: 7.5 ± 2.5 ml/min

Power: 1


220V

3A

Brass roller of diameter (120 + 1) mm and width(50 + 1) mm

Upper surface of the platform covered by a strip of cotton gauze
consisting of 50% of cotton and 50% of polyamide of mass per
unit area (60,5 ± 2) g/m².

Standard Reference

EN ISO 203
44 (7.2)



10.

D
rum

Absorption Tester

Instrument Scope

Determination of the volume loss due to the abrasive action of rubbing a
test piece over a specified grade of abrasive sheet. Method A is for a non
-
rotating test piece and method B for a rotating test pie
ce. For each method,
the result can be reported as a relative volume loss or an abrasion
resistance index

Specifications



Laterally movable test piece holder



Rotatable cylinder to which the abrasive sheet is fixed.



Cylinder diameter of 150 mm ±0,2 mm



Ro
tated at a speed of 40 r/min ± 1 r/min



The test piece holder have a cylindrical opening, the diameter of
which can be adjusted from 15,5 mm to 16,3 mm, and a device for
adjusting the length of the test piece protruding from the opening
to 2 mm±0.2mm.



Weigh
t on test piece: 2.5N, 5N



Length of Drum: 460mm



Abrasion path: 40m/ 20m

Standard reference

BS ISO 4649, SATRA TM 174

Additional requirement

Vacuum cleaner along with instrument

One piece of circular cutting tool and drilling machine



11.

ROSS Flexing Teste
r

Instrument Scope

To test the flex
-
endurance of rubber, sole ,PU etc.


Specifications

No of Grips : 6 sets

Counter: LCD, 0~99,999,999

Temperature: Upto minus (
-
) 20 deg celcius

No of flex: 60±5 cycles per minute

Angle of flex: 90°±2°

Standard re
ference

SATRA TM 60, ASTM D1052, ISO 4643 (annex C)

Additional requirement

Needle or plane type puncher


Annexure I: Technical Specifications for equipment
, Testing Lab, Kanpur


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12.

Full Shoe Water Penetration Tester

Instrument Scope

Used to test the resistance of water and the durability of flexing for
footwear immersed in wate
r.


Specifications

Test Range: UK size for children`s shoe 4~13;for adult`s:1~12

No of test piece holder: 2 pieces

individually detected


Speed: 50~140cpm

Counter: LCD,0~999,999

Angle of flex: 10,15,20,25,30,35,45°

No of flex: 140±10 flex per mi
nute

Dual mode: Both flex resistance & water penetration resistance

Standard Reference

SATRA TM 77 & TM 92





13.

Sole Adhesion Tester

Purpose

To determine the strength of bond for sole adhesion



Specifications



Manual operation.



Analogue readout up to 5
0kg.



Interchangeable toe shapes.



Height adjustable, through adaptor for heel testing.

Standard Reference

SATRA TM 404



14.

Veslic Rub Fastness

Purpose

Determines the effect of dry & wet rubbing produced by a
reciprocating felt pad on the finish of upper and

lining
leather


Specifications



Pre
-
determined counter.



Positional, weighted arm.



Table movement, minimum 80mm.



Cycle speed of 40 rpm.



Weight applied 500g



Finger mass 500g



Sample pad size 15 mm x 15mm

Standard Reference

EN ISO 17700, SATRA TM 173, IUF 45
0, DIN 53339
EN ISO 20344(7.3) ISO 11640


15.

Heel Fatigue Tester

Instrument Scope

This test is used to determine the resistance of medium and
high heels of ladies’ shoes under repeated small impacts to
Annexure I: Technical Specifications for equipment
, Testing Lab, Kanpur


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the heel tip.


Specifications

Impact Energy :0.68J / bl
ow

Impact Frequency :60 blows /min

Adjustable Range of Base Clamp :90mm( H ),80mm( W
),angle 0~180°

Counter LCD,0~999,999

Standard Reference

BS 5131 SATRA TM21



16.

Bennerwart Flexing


Instrument Scope

Used to determine the resistance of materials to

cut growth
during repeated flexing, especially applicable to outsoles
of footwear including sole constructions.

Specifications

No of sample holder: Min 3

Counter : LCD,0~999,999

No of flexes:125
-
150 flexes per minute

Diameter of Mandrel : 30±1mm

Length of Mandrel: 150±1mm

Angle of Flex: 90 ±2°

Standard Reference

SATRA TM `161, ISO 17707



17.

Marking Tester (Scratch Tester)

Instrument scope

This test gives an indication of the resistance of a
footwear material to scuffing, surface damage

which
oc
curs when upper of a shoe is grazed against rough
surface

Specifications

Test angle : 0
-
90 degrees


Weight of pendulum : One kg

Specimen Clamp: Hexagonal

Material of the standard floor : 200x25mm

Specimen base adjustable ring height = 25mm

Stanad
ard reference

SATRA TM 38; SATRA TM 223





18.

Bata Belt Tester

Instrument Scope

This method is intended to determine the resistance of
component or material to crack initiation and growth due to
Annexure I: Technical Specifications for equipment
, Testing Lab, Kanpur


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repeated flexing

Specifications

Belt size : Length:1930±50mm

Width:140±5mm

Sampling : Max.6 pcs

Counter :LCD

0~999,999

Motor : AC1/2HP variable freq.
M
otor

Speed : 247 ±20 rev/ min; 90±8 flexing cycle/minutes

Standard reference

SATRA TM 133

Additional Requirement

Additional belt of cotton canvas

Magnifying glass with scale in mm



19.

Digital Durometer

Instr
ument Scope

To measure the hardness of rubbers and plastics

Specifications



Hand held.



Additional stand available.



Digital display.



Battery operated.



Easily interchangeable modules.

Standard Reference

Applicable to ASTMD 2240, DIN 53505, ISO7619, ISO868



20.

Eyelet Abrasion Tester

Instrument Scope

Used to determine the abrasion statuses of lace via the
standard eyelets under the reciprocal abrasion at a
specified tension

Specifications

Sampling : 6sets

Load

weight)
:
455±5g

Stroke : 76±2mm

Fibreboard

L×W×D

:
25×25×3 mm

Eyelets : ψ4.5 mm

Standard Reference

SATRA TM93




21.

Heel Impact Tester

Instrument Scope

This test is used to determine the endurance of heel of
ladies’ shoe to receive the occasional heav
y blows
during wear.


Specifications

Capacity:

0~18.3J(13.5ft
-
lb ),minimum reading
0.68J(0.5ft
-
lb )

Annexure I: Technical Specifications for equipment
, Testing Lab, Kanpur


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Horizontally Holding Moment of Pendulum:

17.3N~m(12.7ft
-
lb )

Adjustable Range of Base Clamp

: (H )~25mm,angle
0~45°

Standard Reference

BS 5131; SATRA
TM 20



22.

Microscope

Specifications



Carl Zeiss lens



Stand S with column height of 260mm



Stemi mount with drive for column dia 32mm



Dust cover G



Objective 2.0X for higher magnification range
between 16X
-
64X



Trinocular stereo zoom with incident light
illumina
tion



Digital microscopic camera with configuration, tool
and connection cable



23.

Gas Chromotograph Mass Spectrometer System (GC MS)

Column Oven



Accommodates up to two capillary columns



Operating temperature range suitable for all
columns and chromatograph
ic separations. Ambient
temperature +4 °C to 450 °C.



Temperature set point resolution: 1 °C.



Supports at least 9 oven ramps.



Oven cool down 450 to 50 °C in
5

min or less



PPC / EPC control upto 0.01 psi or better



All temperature and time functions should be

microprocessor
-
controlled and shown on the touch
-
screen display of GC.


Programmable Split / Split less Inlet
: 1 nos



Temperature
-
programmable inlet
. Also, Cold
oncolumn injector
.



It should have Oven
-
tracking to simplify working



Heating rate : 50 ˚C to
400

˚C in 1 ˚C increments



Heat
-
up rate of 1 ˚C/min to 200 ˚C/min or ballistic



Cool down rate : 380 ˚C to 50 ˚C in less than 5
minutes



Ramps:3

or better

Back flushing, & MS Vent Devise
(from OEM):


Back flushing

to increase the column life by removing
un
wanted eluents and
MS Vent
(or equivalent
technology) to change the
column without venting
Annexure I: Technical Specifications for equipment
, Testing Lab, Kanpur


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vacuum

Mass Spectrometer



Mass
range:

1
-

1000
amu
or better



Scan speed :
5000

amu/s

or better



Source
Temperature:

50 ˚C


3
00 ˚C or
higher



GC transfer line: Setta
b
le 50 ˚C


30
0 ˚C

or higher



EI full scan sensitivity : S/N 800:1 or more for 1 pg
OFN



True Simultaneous SIM and SCAN



Ion Source
design:

Ion Source should have
simplified design for easy maintenance and change
of EI to CI. Opening of ion source should be t
ool
free
.



Filament:

long life filament
. Preferably dual
-
filament type

Auto Samper with least
50

vials
capacity or more




Operated through GC software & injection Volume
linearity
should have

99% correlation



Area
Reproducibility:

0.3% RSD



Single
auto samp
ler

should do injections in both
injector ports without any hardware
change.


Chromatographic Data Software:


Single point control of GC
-
MSD system and its
modules, customizable reports, GLP features should
also have

software for data acquisition, control
,
chromatographic data evaluation, reporting sequencing.
Licensed Software should be supplied with the system.

Library

NIST (latest edition)

Columns: 4




5%
-
phenyl column based on diphenyl
methylsiloxane
chemistry,

30 m
X
0.2
4
mm id

X

0.25u film thickne
ss
-

2 nos



(35%
-
Phenyl)
-

methylpolysiloxane

column, 3
0 m

x
0.24mm x 0.25µ film thickness

: 2 nos


All the instrument modules should have PPC / EPC
control.

Accessories

PC & PRINTER( 19” Monitor, i3 or above)


24.

Quartenary HPLC System

Pump



Eluents: 4




No. of pumps : 1

Annexure I: Technical Specifications for equipment
, Testing Lab, Kanpur


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14




Flow : 0


5

ml/min

or more



Accuracy :
0.5%

or better




Precision : 0.3%

or better



Pressure range :
5000
psi
around



Gradient forms : Linear

PDA Detector




Wavelength range : 190


700 nm

or better





Wavelength accuracy : ±1 nm



Bandwidth : 5 nm

or better




No. of diodes : 512 or above



3D, peak purity and spectral information should be
present & operational.

Auto sampler

:




Injection Volume : 2


200 ul



Precision : 0.3% RSD

or better



Car
ryover : 0.005%

or better



Tray capacity :
Desirably
50

nos x 2 ml vials



Pressure: 6
0
00 psi

or better

Column Compartment :




Ambient to 90
o
C



Temperature stability

:


±0.2 ˚C

or better



Temperature repeatability

:


±1 ˚C

or better

Software:


Single poin
t control for all HPLC modules.
Customizable report formats. Capable of doing
integration, calculations.Software should have GLP
features


Columns

End capped
C
-
18, 150x4.6 mm,
4

to
5

microns
: 4 nos
with guard columns

(20 no.’s)


Latest configuration PC &
printer( 19” Monitor, i3 or
above)


25.

AAS (Atomic Absorption Spectrometer)




Should include 190
-
890

nm wavelength range.



Should have capability of
4 or More

lamps turrete



It should have capabilities to control through PC .
Annexure I: Technical Specifications for equipment
, Testing Lab, Kanpur


Page
15


Full control software should be qu
oted optionally.



One or more turret for lamp mounting with
provision
for

at least one EDL/Super lamp
mounting provision



Built
-
in Power supply for High Efficiency
EDL/Super lamps.



D
2

background correction with electronic
modulation and automatic attenuatio
n.



True double beam Echelle optics
/Holographic
grating

with 1800 liner
.



High efficiency, segmented Solid State
detector
/PMT



Capability for

Automatic

alignment of lamps.
Instantly/automatically recognizes and s
ets up the
wavelength, slit,
lamp parameters &
automatically
aligns the lamp.



Automatic Method saving/instrument will
automatically be ready to run.



Single element HCL

of (Pb, Cd, As, Cr, Cu, Co,
Ni, Zn) & EDL of (As, Pb)


Optional Accessories to be supplied
by AA Manufacturer only & not
Local



HCL
Lamps

(Single élément): Al, As, Cd, Co, Cr,
Cu, Fe, Hg, Ni, Pb
, So, Bam Sn, Ti, Zr, Se
.



Air Compressor
,

Air/Acetylene Filter unit &
regulators, N
2
O Regulator with Pre Heater,

gas box
etc.



10
-
cm single
-
slot solid titanium burner head for
air/acetylene

& Bu
rner Head for N20



Hydride generator accessory for analysing As, Sb,
Hg and Sn

with suitable spray accessories to AAS
end.

Software

Easy method development, complying to quality
protocols and compliance

Also quote

Branded PC & Printer
( 19” Monitor, i3 or

above)


26.

LCMS


Single Quadrupole LC/MS system ideally suited for
both Qualitative and Quantitative analysis. The system
should be capable of capturing minimum 2 signals, one
from MS and another from any HPLC
-
DAD

detector
connected.

Mass Range

up to
200
0 or more
m/z

Interface

Simple Interface should be capable of maintaining
cleanliness of ion optics and optimized for ion de
-
clustering, capable of handling large batches of
Annexure I: Technical Specifications for equipment
, Testing Lab, Kanpur


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16


complex samples without performance degradation or
need of maintenance. The inte
rface should be capable
of ambient temperature operation to maintain structural
integrity of thermally labile and fragile molecules.


Nebulization Probe

Easily removable pneumatically assisted Grounded
Nebulizer Probe (without any fittings) and should b
e
angular towards Capillary entrance. The Probe should
be adjustable in X and Y


axes. Pneumatic control of
nebulizer pressure should be
preferably
through
software.

Desolvation assembly

It should consist of capillary & counter or dry gas with
tempera
ture control upto 300deg C or above through
software for better desolvation capabilities.

The following features
should be available



Decoupled technology for adjusting voltages .



Tool free design for easy removal of the
capillary.



Pre Quadrapole (before th
e main analyzing
quad) for filtering unwanted masses.


Ion Source: (ESI)

Ion sources should be compatible to work with Polar
and mid polar compounds, along with compatible
housing, probes and interface kits wherever required.
Drying gas, provision in the
system for best desolvation
must be present, which can be controlled by software


Inlet Modes

Along with

HPLC eluent connection into MS; a
External or Built
-
in Syringe provision for direct
infusion facility is required to operate MS in standalone
mode als
o

Sensitivity

Signal to noise ratio must be specified
for
both positive
and negative modes for ESI.


a.

ESI


SIM (positive mode) : 1 pg/ ul reserpine
should give s/n ≥ 120:1
or better

b.

ESI


SIM (negative mode) : 2 pg/ ul P
-
nitrophenol

or a comparable comp
ound

should
give s/n ≥ 100:1
or better

Vacuum System

A robust high efficiency 2 or 3 stage Turbo Molecular
pump vacuum system with minimum maintenance and
utility requirements.

Quadrupoles

Equipment must be equipped with
Quadrupoles

having
high standa
rds of mass stability in varying lab
temperature conditions with facility for excellent
focusing of ions into the Quadrupoles for high
Annexure I: Technical Specifications for equipment
, Testing Lab, Kanpur


Page
17


sensitivity and resolution to simplify tuning and
maximize analyzer efficiency.

Mas scan speed/ Rate

The system should

have scan speed / rate of minimum
5000
u / sec with sufficient resolution
.

Dynamic Range

System should have a dynamic rate of
10 e
5

or better

Resolution


Better than unit mass i.e. M/δM≥M, MFWH (Full
width Half Height) ≤ 0.7 ± 0.1 amu over the entire
mass range 20


3000 amu.

Mass Accuracy

± 0.1 amu or better / 24 hr; ± 3
0
C

Mass Axis Stability

±
0.1 amu or better / 24 hr; ± 3
0
C

Operating modes

Manual
and automated instrument optimization,
automated instrument calibration and resolution
optimization (Autotuning).


HPLC

A)

Quaternary Pump

i)

Flow : 0


5

ml /min
or higher

ii)

Back Pressure :
50
00 psi
or better

iii)

Accuracy : 1%

or better

iv)

Uni direction piston movemen
t design

v)

G
radient profiles

in particular should have
linear


B)

PDA Detector

i)

Wavelength range : 190


700 nm

or better

ii)

Wavelength accuracy : ±1 nm

iii)

Bandwidth : 5 nm

or better

iv)

No. of diodes : 512 or above


C)

Auto Sampler :

i)

Sample capacity :
20 or more vials

ii)

Inje
ction volume : 0


100 ul

iii)

Cross contamination : 0.005%

or better


D)

Column Compartment :
Heater : up to 90
o
C


Software

Should have single point control for all MS and HPLC
modules. Should have capability for presentable
reports. Ability to do calculations
& drawing
calibration curves.

Windows based latest version

Computer platform

PC of any make HP / DELL / Lenovo with

the latest
(XP or 7) Windows

operating system with all required
software and controls. Latest configuration.

Gas generator


A Nitrogen ge
nerator
(either with inbuilt air
compressor or a separate suitable air compressor)
suitable for the LCMS should be supplied.

Columns


Endcapped
C
-
18, 150x2.2 mm, 1.8u : 4 nos with guard
columns



20no.’s

Annexure I: Technical Specifications for equipment
, Testing Lab, Kanpur


Page
18



PC & Printer ( 19” Monitor, i3 or above)



27.

Gas
Chromotograph

-
ECD

Column Oven




Accommodates up to two capillary columns



Operating temperature range suitable for all
columns and chromatographic separations. Ambient
temperature +4 °C to 450 °C

or better
.



Temperature set point resolution: 1 °C

or better
.



Supports at least 9 oven ramps.



Oven cool down 450 to 50 °C in
5

min or less



PPC / EPC control upto 0.1 psi or better



All temperature and time functions should be
microprocessor
-
controlled and shown on the touch
-
screen display of GC.



Back flushing

Progr
ammable Split / Split less Inlet
: 1 nos.( To separate Low boilers &
High boilers)




Temperature
-
programmable inlet



It should have Oven
-
tracking to simplify working



Heating rate : 50 ˚C to
4
00 ˚C
or higher
in 1 ˚C
increments



Heat
-
up rate of 1 ˚C/min to 200 ˚C/min or ballistic



Cool down rate : 380 ˚C to 50 ˚C in less than 5
minutes



Ramps: 3 or more

ECD: Electron Capture Detector




Source :
15 mCi
Ni

63



Working t
empera
ture

:
35
0

˚C
or more
by software

Sensitivity :
< 0.05 pg per chloroethylene
/
Lindane

with argon/methane or nitrogen



Signal frequency :
200, 800 m/sec

Chromatographic Data Software

Single point control of GC
-
MSD system and its
modules, customizable repor
ts, GLP features should
also have

software for data acquisition, control,
chromatographic data evaluation, reporting sequencing.
Licensed Software should be supplied with the system.

Auto Injector with least 100 vials
capacity or more


Operated through GC

softwar
e & injection Volume
linearity should have
99% correlation and Area
Reproducibility RSD 0.3%

or better
.

The injector should be able to do injections in case
there are 2 injection ports.

Columns



5%
-
phenyl column based on diphenyl
methylsiloxane che
mistry ,
30

m

x 0.2
4
mm

i.d.

x
0.25
µ

film thickness
:
-

2 nos



(35%
-
Phenyl)
-

methylpolysiloxane column,
30

m
x
0.2
4
mm x 0.25µ film thickness
: 2 nos

Annexure I: Technical Specifications for equipment
, Testing Lab, Kanpur


Page
19



All the GC modules should have
EPC / PPC control.


Accessories

:
PC & PRINTER

( 19” Monitor, i3 or
above)



28.

Gas Chromatograph

MS

-

FID

Column Oven




Accommodates up to two capillary columns



Operating temperature range suitable for all
columns and chromatographic separations. Ambient
temperature +4 °C to 450 °C.



Temperature set point resolution: 1 °C.



Supports
at least 9 oven ramps.



Oven cool down 450 to 50 °C in
5
min or less



PPC / EPC control upto 0.1 psi or better



All temperature and time functions should be
microprocessor
-
controlled and shown on the touch
-
screen display of GC.



Back flushing
.

Programmable S
plit / Split less
Inlet:

2 nos.




Temperature
-
programmable inlet



It should have Oven
-
tracking to simplify working



Heating rate : 50 ˚C
to
400

˚C
or higher
in 1 ˚C
increments



Heat
-
up rate of 1 ˚C/min to 200 ˚C/min or ballistic



Cool down rate : 380 ˚C to 50 ˚C in less than 5
minutes



Ramps: 3

or more.


Flame Ion detector(FID)




Automatic Flame
-
out detection should be p
ossible.



The minimum detection limit should be < 3 pg
carbon/sec as propane /


nonane



Should suit for working temperature of 350°C or
higher.


Mass Spectrometer




Mass range : 1
-

1000
amu
or higher



Scan speed :
5000
amu/s

or better



Source Temperature :
50 ˚C


350 ˚C,



GC transfer line: Settable 50 ˚C


3
0
0 ˚C

or better



EI full scan sensitivity : S/N 800:1 or more for 1 pg
OFN



True Simultaneous SIM and SCAN



Ion Source design :
Ion Source should have
simplified design for easy maintenance and change
Annexure I: Technical Specifications for equipment
, Testing Lab, Kanpur


Page
20


of EI

to CI. Opening of ion source should be tool
free.



Filament : long life filament

Chromatographic Data Software:


Single point control of GC
-
MSD system and its
modules, customizable reports, GLP features should
also have

software for data acquisition, cont
rol,
chromatographic data evaluation, reporting sequencing.
Licensed Software should be supplied with the system.

Auto Injector with least 100 vials
capacity or more




Operated through GC software & injection Volume
linearity is 99% correlation and Area
Re
producibility RSD 0.3%

or better
.



The injector should be able to do injections in case
there are 2 injection ports.

Columns: 4




5%
-
phenyl column based on diphenyl
methylsiloxane chemistry,
30 m x 0.2
4
mm
i.d.
x
0.25
µ

film thickness

-

2 nos



(35%
-
Phenyl)
-

me
thylpolysiloxane column,
3
0 m

x
0.2
4

mm/id x 0.25µ film thickness

: 2 nos


All the GC modules should have EPC / PPC control.

Accessories

PC & P
rinter

( 19” Monitor, i3 or above)


29.

UV
-
Vis Spectrophotometer

Optics


True
Double
-
beam, sealed, quartz
-
coated
mirrors; lens
-
free system to reduce chromatic aberrations


Wavelength range

190
-
900
nm
or more

Bandwidth

1 nm
&
Variable

Stray light


a)

At 220 nm (NaI) < 0.01%T

b)

At 340 nm (NaNO
2
) < 0.01%T

c)

At 370 nm (NaNO
2
) < 0.01%T

d)

At 200 nm (KCl) < 1%T

Wavelength ac
curacy

±0.1 nm

or better

Wavelength Reproducibility

±0.05 nm

or better

Photometric stability

< 0.00015 A / hr

Photometric noise at 500 nm (RMS)

< 0.00005 A

Annexure I: Technical Specifications for equipment
, Testing Lab, Kanpur


Page
21


Baseline Flatness (Abs):

± 0.001 Abs

Source

Deuterium and Tungsten pre
-
aligned sources with

automatic switch
-
over

Accessories

a)

PC & Printer ( 19” Monitor, i3 or above)

b)

2 pair quartz cuvette

c)

Glass cuvettes:
-

1cm, 2c, & 4 cm path length

d)

Cell Holder for holding cell upto 5cm length


30.

pH Meter specifications

S
cope

Digital Bench top pH / ion meter
with TFT complete
with high performance combination electrode, one
electrode stand with arm, standard automatic
temperature compensation, probe and also facility for
manual temperature compensation, electrode storage
bottle, power adapter, instruction man
u
al and service
manual confo
rming to international standards

Technical Features

Bench top ion meter includes all pH basics and
simultaneous display of pH, mV and temperature with
water resistant membrane key pad.

• Calibration fast and accurate using auto

calibration
with built
-
in auto buffer recognition of three buffers
and custom buffer values can be entered for accurate
measurement over the entire pH range.

pH range

1
-

14

Resolution: pH

0.1 freely selectable

or better

Accuracy


+/
-

0.002

Ion Concen
tration


0.000 to 1000.0 %

0.000 to 10000.0 ppm

1.00E
-
9 to 9.99E+9 mg/L

1.00E
-
0 to 9.99E+9 mmmo/L

Annexure I: Technical Specifications for equipment
, Testing Lab, Kanpur


Page
22


1.00E
-
9 to 9.99E+0 mol/L

Temperature (MTC) compensation

Should be available for
-
10°C to

60°C or better

Resolution


0.1 °C

Temperature Compensation

Both a
utomatic (ATC) and manual (MTC)

Display

Big TFT screen

Language display


English

GLP features

sample ID, sensor ID, user ID and meter ID Lab
Manager’s Menu protected by PIN code


Data logger and alarms selectable Buffer solutions : 5
set of pre defined

buffers + 1 freely definable by user
Calibration : 1 to 5 points Inputs : BNC input for
measuring and combined electrode, 1 input for
reference electrode, 1 input for temperature sensor
(Pt1000 pr NTC30K)

Outputs

Bi
-
directional RS232C interface for print
er or PC,
analog output, Possible USB and RS232 interface

A
ccessories

• Glass pH electrode with electrode holder

• Fluoride Electrode with cable

• Reference Electrode with cable

• Reference electrode

• Electrode cable with BNC connector

• Cable for refere
nce electrode

• Stainless steel ATC probe NTC30K

• Set of buffer solutions:

Sachet pH 4.01

Annexure I: Technical Specifications for equipment
, Testing Lab, Kanpur


Page
23


Sachet pH 7.00

Sachet pH 9.21

Calibration

Manufacturer/ vender has to provide certified reference
material having National/international traceability

Power require
ment

220/240V, 50Hz.



31.

A.

Mechanical Shaker

(Type I)

31. B. Mechanical Shaker (Type II)

Specification

Type I

-

Reciprocating type with microprocessor
control system


Type II
-


Orbital Shaking type

Timer

Upto 60min or continuous operation

Shaking ampli
tude

30mm

Shaking frequency

20 to 300 rpm

Electrical connection

230v 60Hz, 65W



Accessories for Mechanical Shaker

Shaking Tray

Made of Stainless steel with holes to accommodate
clamps for separating funnels, flasks and test tube racks

Universal Mount

For secure attachment of different shaking objects

Clamp

250
-
300ml Erlenmeyer flask

Clamp

For 500ml separation funnel



32.

Ultrasonic Bath

with Digital timer, Heater, Degas & Temperature Monitor
with tank cover, perforated tray and solid tray

Specification
s



Power 40 Hz



Temp. Range:
-

80°C
+
1°C



SS 3041 stainless steel tank

Tank Capacity

Around 6 litres

Drain

Yes

Power

230/240V


33.

Microwave Digestion System

MAGNETRON

The microwave system should have Dual Magnetron
System with diffuser for homogeneous microwa
ve
Annexure I: Technical Specifications for equipment
, Testing Lab, Kanpur


Page
24


power distribution in the cavity. The Microwave power
of Microwave

Digestion System should be 1600 Watt
or higher and the delivered power should be 1400Watt/

min controllable via microprocessor ± 1W increments.


System should have a camera system to see

the live
images of the inside of the cavity during

digestion.


SAFETY

The system should have good interlocking system for
safety and cavity door should

have safety interlock.


EXHAUST

The system should have inbuilt exhaust system to cool
the vessels and

to drive

away if any fumes in the cavity.


VESSELS

The Microwave Digestion System should have
provision for high throughput
;

it should be possible to
digest atleast eight samples or more simultaneously
using
high

pressure vessels in single operation. The

volume

of

pressure vessel should be about 100ml and it
should be designed to withstand up to temperature
300ºC and pressure 100 Bar or more.

There should be an internal temperature probe for real
time temperature measurement inside the reaction
vessel. Ve
ssel should have vent and reseal
p
rovision

CONTROLLER

System should be controlled by a color touch screen
controller, which should have method storage capacity
of 100 methods or more.




34.

Bacteriological Incubator

Size

450x450x450mm

Tempera
ture range

Amb
ient to 60 degree

Temperature controller

PID Digital tempera
ture controller with calibration
certificate

Accuracy

0.5

degree centigrade





35.

Ageing Chamber

Capacity

8 cuft humidity chamber (Ageing Chamber)

Temperature Range

+
50
degree c to 100 degree c (±1

degree after
stabilization
)

Humidity Range

10
% to 95% RH over the temperature range of +
50

to +
Annexure I: Technical Specifications for equipment
, Testing Lab, Kanpur


Page
25


80 degrees by a +3 degree c dew point. ±3 % RH
typically after stabilization

Sensor

PT
-
100 3lead RTD for temperature and dry capacitance
type humidity sensor

Features

1.5mm, SS 304 grade stainless steel interior

Urethane/fiberglass insulation

Refrigeration pressure tap & gauges

Power supply

230v, 1ph, 50Hz



36.

Vacuum Pump


Heavy duty


S/E stage

Capacity

50 lts

Maximum flow

27 inches per mercury



37.

Rotary E
vaporator

with suitable vacuum pump and chiller

Specification

Motorized lift with provisions for automatic lifting of
the flask in case of power failure.

Rotation speed up to 280 rpm or better with
microprocessor control.

Digital Display for Rotation Speed

and Vapor
Temperature.

Digital bath temperature display of both set and actual
temperature simultaneously with microprocessor
control ranging from ambient to 180 deg C with an
accuracy of ± 2 deg C.

Automatic over heat cut
-
off protection

Evaporating flask

from 50
-
2
000 ml can be used on the
same joint adapter without additional connections.

Vertical Glass Assembly.

(100ml
-
12 no.’s; 250ml
-
12 no.’s)

1
litre
/500ml

Evaporating Flask
s

and Receiving Flask
1
litre capacity
should be provided in standard scope of

supply.

All display parameters like water bath temperature,
vacuum etc. should
be available.

All glass components should be made of Borosilicate
Annexure I: Technical Specifications for equipment
, Testing Lab, Kanpur


Page
26


glass.

All connections (for vacuum, water circulation etc.)
should be at the lower part of the condenser.

Shou
ld be supplied along with woulff bottle.


Vacuum Controller

Modular (not integrated) vacuum controller with
control knob and large graphic display screen.

Integrated solvent database of 43 solvents for
convenient setting of distillation conditions.

Spee
d control for vacuum pump.

Measuring range: 1400
-

0 mbar

or better
.

Control range: 1100
-

1 mbar.

Integrated aeration valve and precision pressure sensor.

Timer function for process termination after pre
-
specified time

All controls for the Rotavapor e.g.
, lifting /lowering of
the evaporating flask, Rotation start/stop should be
controlled via the vacuum controller.

Provision for display of Chiller temperature and
control.

Vacuum Pump

Single stroke Speed control vacuum pump with a flow
rate of 1.8 m
3
/h

o
r better
.

Ultimate vacuum


less than 10 mbar

2 stage diaphragm made of PTFE

Visual inspection of diaphragms for checking solvent
build up and contamination.

Soundproofing with enclosed housing to minimize
noise and vibrations

Re
-
circulating Chiller


Co
mpact and Robust Re
-
circulating Chiller with a
cooling capacity of 500 Watts at 15 deg

Temperature Range:
-
10 deg c to 25 deg C

Pump Capacity: 3 liters/min at 0.6 bar

Coolant: CFC Free

Suitable enough to control two rotary evaporators.

The equipment should

be provided with following
additional spare parts:



Stop Cocks NS 18.8/38


1 No.

Annexure I: Technical Specifications for equipment
, Testing Lab, Kanpur


Page
27




Vapor Duct SJ 29.2.32 & Clip

1 No.



Gasket





2 Nos.



Evaporating Flask 500 ml


1 No.



Evaporating Flask 2000 ml


1 No.



Evaporating Flask 250 ml 10 Nos.



Evapor
ating Flask 100 ml 10 Nos.



Control Cable RJ45



1 No.



38.

Nitrogen Evaporator

Specifications



System should be controlled by Microprocessor



Sys
tem able to control individual

manifolds.



System
to be
equipped with adjustable nitrogen
regulat
or (from 4
-
25psi) and gauge.



Should have
Sensor Endpoint technology



At least
6 Positions should have
suitable
Unattended
operation



System able to handle two different tube size rack
1ml to 200ml

or better.



Vortex Shearing Technology



System equipped with te
mperature controlled water
bath (Ambient to 99
o
C).



User Friendly Displays and Diagnostics



Dial
-
in
-
time, temperature and time, temperature
readouts.



Fit on any laboratory bench with a small footprint.



When not in use, provision for capping of positions
shou
ld be there for nitrogen saving.

39.

Electrical Resistance Tester

Instrument Scope

Measurement of electrical resistance for anti static and
conductive safety, protective and occupational footwear

Specifications



50gm of suitable silver based conductive lacque
r



4 kg of 5mm diameter stainless steel balls (ISO
3290) to act as internal electrode



Resistance measuring meter



Resistance measuring board



Copper contact plate (External electrode)

Standard reference

EN ISO 20344.5.10



40.

Electrical Insulation Teste
r

Instr
ument Scope

This standard is applicable to electrically insulating
Annexure I: Technical Specifications for equipment
, Testing Lab, Kanpur


Page
28


footwear used for working live or close to live parts on
insulation exceeding 1000V a.c

Specifications

Test Voltage

: Voltage withstanding AC:0~5KV adjustable

Cover Current

:0.5,1,3,5,10
mA 5(stages)

Impedance

:
500V DC/250MΩ

Test Method
: Automatically determines the fallure
specimen

Test Period:

Voltage withstanding: Manual or
auto(Time:0~180sec)

Failure Indicator

: Lamp & buzzer

Accessory

High pressure test probe

Power

1

,AV220V,3A

Standard reference

AN
SI Z41, CSA
-
Z195, GB 12011, BS EN 50321



41.

Heat Insulation Tester


Instrument Scope

This tester is used to determine the heat insulation performance for
the whole shoe.

Specifications

Sand Bath Size

: (40±2)cm×(40±2)cm the height at least 5cm

Sand Volum
e

: 5000 ± 250 cm3

Sand Granular Size

: 0.3~1.0mm

Temperature of Hotplate

: Room temp.~150° ± 5° or 250° ± 5°

Heating Power Consumption

: 2500 ± 250W and over

Power

: 1§

220V

Standard Reference

EN ISO 20344 (5.12)







42.

Cold Conductivity of Footwear


Instrument Scope

To assess the
cold

insulation properties of footwear

Specifications



Adjustable height table for sample mounting.



Incorporated within freezer unit.



Temper
ature to
-
20 degrees C. [subject to ambient]



LCD display.

Standard reference



EN ISO 20344(5.13)



43.

Ankle Protection Tester

Annexure I: Technical Specifications for equipment
, Testing Lab, Kanpur


Page
29


Instrument Scope

To assess the shock absorption properties of ankle
protective materials

Specifications

To be supplied with calibra
tion certificate

Power consumption of 450W

Noise of 70 db

Power supply of 220 V.AC.

Standard Reference

EN ISO 20344:5:17




44.

Heat Resistance Tester

Instrument Scope

For upper leather & soling material, used to determine
the amount of visible damage due to

short term contact
with heat.

Specifications



Heated block 25mm x 25 mm



Contact pressure 20kPa.



Guarded heated element.



Maximum temperature 300 degrees c.



Digital display.



Lifting handle.

Standard Reference

EN ISO 20344(8.7)



45.

Slip Resistance Tester

I
nstrument Scope

A machine to determine
co
-
efficient of
friction

between
shoe sole
material
and
standard floor surfaces.

Specifications



Embeded Industrial PC Operation system that
automatically calculates and displayes coefficient
of friction reading and d
isplays graphical
representation of relevant data



Computer controlled operation.



Electric motor featuring clutch.



Displayed result, C.O.F figure.



Force/movement traces displayed with option to
print.



Interchangeable test surfaces.



Adjustable load/speed par
ameters.



Independent tarring procedure.



Vertical/horizontal loadcells incorporated.



Adjustable sample positioning.



Pneumatic cradle operation.

Standard Reference



EN ISO 13287; SATRA TM 144




Annexure I: Technical Specifications for equipment
, Testing Lab, Kanpur


Page
30


This shall also be supplied
complete
with the


Calibrated Flo
or Quarry Tiles


Specifications

o

Certificate of calibration required

o

Size of tiles 15x15x1.2 cms


Surface Roughness Meter


Specifications


o

A hand held instrument for measuring the Rz
surface roughness of either the plate or the ceramic
tile used for EN tes
ting to ensure it meets the
required roughness in accordance with the standard


Stainless Steel


p呄⁆汯潲


p灥c楦楣a瑩潮o


o

The stainless steel standard floor is a requirement
for EN 13287 and for safety foot ware testing with
suitable instrument size 50
x15cms


PRS Lasts


C桩h摲d湳n 獩se ㈠ 瑯t
a摵汴‱


p灥c楦楣a瑩潮o


o

Required to support the specimen shoe during
testing

o

To withstand the reverse breaking loads during
testing

o

Full range of 26 pairs consists of lasts from children
to adult


Calibrated Stan
dard Rubber


Specifications


o

Used to calibrated standard rubber slider is supplied
with calibrated certificate

o

Same material can be used for EN 13287


ENL 13 Pairs European sizes 36
-
48


Specifications


o

Suitable for testing EN13287 and is required to
suppo
rt the specimen during testing

o

To withstand the reverse breaking loads applied
during testing

o

European adult size 36
-
48




46.

De Mattia Flex


Instrument Scope

Instrument designed to carry out dynamic flexing test on coated fabric or
rubber test piece

Annexure I: Technical Specifications for equipment
, Testing Lab, Kanpur


Page
31


Specif
ications

Sample holder:
3

sets

Grip Space (max): 75 mm

Counter

: LCD, 0~999,999

Stroke Length: 57 ±0.5mm

Frequency: 5,0 Hz ± 0,2 Hz.

Standard reference

ISO 7854 Method A



47.

Corrosion Resistance Salt Spray Tester

Instrument Scope

U
sed to test the
anti
-
cor
rosion quality of the surface of all materials
after the rust
-
proof of painting, coating, electroplating, anoding and
rust
-
proof of greasing

Test Chamber

270
Litre

Temp.

Test

NSS.ACSS 35
°C

±1

/ CASS 50


±1


Air

NSS.ACSS 47
°C

±1

/ CASS 63


±1


Interior
Dimension(W×D×H)

90×60×50 cm


Test water

25 Litre

Power

1
§
,AC220V,20A

Stanadard reference

ASTM B117 ISO 9227



48.

Rotary blade cut tester

Instrument Scope

A machine to measure the cut resistance properties of samples

Specifications



Interchange
able sample holders.




Magnetic location.




LCD display of cycles.



Automatic stoppage after blade penetrates the last sample




Automatic cut out on sample failure.




Count mechanism =1/10 cycle.




Blade under applied load.




Loading Pressure : 5 N ± 0.05 N




Blad
e size : Ø 45 ± 0.5 mm ,3 mm in thickness




Cutting Travel: 50 mm




Cutting speed : 10 cm/ sec




Counter : 199999.9




Two specimens holder




Major parts to be made of stainless steel

EN388

Standard Reference

EN 388


Annexure I: Technical Specifications for equipment
, Testing Lab, Kanpur


Page
32


49.

Water Purifier for HPLC / LC
-
MS mobile phas
e and for lab reagent
preparation
.

Specifications

The tap water should pass through a prefilteration unit comprising of
5 & 1 micron filter & a booster pump.

The water purification system
should

deliver pure(Type II) &
ultrapure water (type I)directly fro
m tap water
so as

to eliminate the
need of two different systems in the same laboratory

The system shall be comprised of a single water purification unit
containing reverse osmosis, electro
-
deionisation with carbon beads
on cathode, uv irradiation (for bot
h type 1 & Type II) ion
-
exchange
and activated carbon technologies on cathode and polishing device.

To eliminate the need of deionization cartridges regular replacement,
the water system will include an EDI (ElectroDeIonisation) module
that does not requir
e softening pre
-
treatment.

The built
-
in TOC monitor

(range 1ppb
-
999ppb) should be present.

The ultrapure water system will have a built
-
in UV lamp with
emission at 185 and 254 nm wavelength.

The system should be able to take feed

water upto 2000 microS/cm

&
free chlorine of 3 ppm.

A 30 liter reservoir should be provided.

The ultrapure water delivery should be from an independent
dispenser displaying the water parameters like TOC, Resistivity,
volume of water dispensed etc.

The system should produce water o
f the following quality

Type II Type I

Resistivity: > 5 typically Resistivity: > 18.2 typically

TOC : < 30 ppb TOC

: < 5 ppb

Flow rate: 3 lit/hr
Bacteria : < 1cfu/ml.


Conductivity

: < 0.055 uS/cm


Flow Rate: upto 2 lit
/min

The output from water system should be fed to additional attachment
for providing


ultrapure water with extremely low levels of elemental
Annexure I: Technical Specifications for equipment
, Testing Lab, Kanpur


Page
33


contamination (ppt or sub
-
ppt level) from ultrapure feed water system
for ICP MS application.

Before the delivery

point
,

system should be accommodated with
0.1micron charged durapore membrane filter to avoid the risk of trace
elements/particles.

The system should accompany a long tubing to deliver water directly
to the laminar hood and a glass holder to hold the tubi
ng.

Essential water quality information should be clearly visible at the
point of delivery.

There should be no metallic parts in the system
,

delivering water to
the laminar flow hood.

Should accompany a footswitch for water delivery, reducing the risks
of
external contamination, as scientists do not need to remove their
hands from a laminar flow hood.





50.

Nickel Apparatus

Specifications


Rotation Apparatus

Vertical tumbling barrel

3 layer aluminium retaining assembly

2 layer PMP retaining assembly

Granulat
e for test EN 12472

Cutting paste for test EN 12472

Reference disk for EN 181D



51.

Hot Air Oven

Inner and Outer


SS 304 & MS powder coated

Accuracy

±1 degree centigrade

Temp. Range

100°C or more

Annexure I: Technical Specifications for equipment
, Testing Lab, Kanpur


Page
34


Temp controller

Digital

Temp uniform

Air circulation fan



52.

Disperse
r





Plastics in contact with media consist of high
-
purity materials
such as PTFE, ETFE, FEP, and PFA.

The purest sapphire is used for replaceable valves. Depending on
the application, platinum
-
iridium or tantalum are available as
spring materials
.



The 45 mm standard thread plus the included adapters fit most
common lab bottles.



The valve block can be rotated 360° so that the bottle label
always faces the user for safety.



Telescoping filling tube adjusts to different bottle sizes



Easy disassemb
ly for replacement of the dispensing cartridge
\



The volume range is from 1ml to 10ml



53.

Mantle & Hot Plate


Specification

MS Top & survive control



54.

Chiller


Specification

20 lit tank, pump and thermostat with temperature display



55.

Vacuum Manifold

Specif
ication



Should be able to speed up the sample preparation by
processing up to 24 samples simultaneously



3/8 “ i.d tubing to connect the valve to the vacuum
source


56.

UHPLC (
High Pressure Binary Gradient HPLC)

Pump



Eluents: 2

No. of pumps : 1 with
atleast

2 valves

Flow : 0.001


5 ml/min

or better

Annexure I: Technical Specifications for equipment
, Testing Lab, Kanpur


Page
35


Accuracy : 0.5%

or better

Precision : 0.075%

or better

Pressure range : 14000 or more psi for entire flow rate range (0


5
ml/min)

PDA

Wavelength range :

190
-
700 nm

or better

Noise: ±0.9 x 10
-
5

AU

or better

Dri
ft: 0.7 x 10
-
3

AU/hr

or better

Linear dynamic range : ≥ 1.8 AU with <5% deviation

No. of diodes : 512

or more

3D, peak purity and spectral information should be present &
operational.

Autosampler

Injection Volume : 2


500 ul
(should include this range)

Pr
ecision : 0.3% RSD

or better

Carryover : 0.005%

or better

Tray capacity :
50 no. or more


Column Compartment

Ambient to 90
o
C

Temperature stability

:


±0.2 ˚C

Temperature repeatability

:


±1 ˚C


Software

Single point control for all HPLC modules. Cust
omizable report
formats. Capable of doing integration, calculations, 3D & peak
purity studies.


Columns

End capped C
-
18, 150x4.6 mm, 2mm or less

: 4 nos with guard
columns: 20no.’s



Latest configuration PC & mono Laserjet printer
( 19” Monitor,
i3 or a
bove)